Phosphorus-31 NMR Spectroscopy

Phosphorus-31 NMR Spectroscopy
Author :
Publisher : Springer Science & Business Media
Total Pages : 138
Release :
ISBN-10 : 9783540791188
ISBN-13 : 3540791183
Rating : 4/5 (183 Downloads)

Book Synopsis Phosphorus-31 NMR Spectroscopy by : Olaf Kühl

Download or read book Phosphorus-31 NMR Spectroscopy written by Olaf Kühl and published by Springer Science & Business Media. This book was released on 2008-08-22 with total page 138 pages. Available in PDF, EPUB and Kindle. Book excerpt: Nuclear Magnetic Resonance is a powerful tool, especially for the identification of 1 13 hitherto unknown organic compounds. H- and C-NMR spectroscopy is known and applied by virtually every synthetically working Organic Chemist. Con- quently, the factors governing the differences in chemical shift values, based on chemical environment, bonding, temperature, solvent, pH, etc. , are well understood, and specialty methods developed for almost every conceivable structural challenge. Proton and carbon NMR spectroscopy is part of most bachelors degree courses, with advanced methods integrated into masters degree and other graduate courses. In view of this universal knowledge about proton and carbon NMR spectr- copy within the chemical community, it is remarkable that heteronuclear NMR is still looked upon as something of a curiosity. Admittedly, most organic compounds contain only nitrogen, oxygen, and sulfur atoms, as well as the obligatory hydrogen and carbon atoms, elements that have an unfavourable isotope distribution when it comes to NMR spectroscopy. Each of these three elements has a dominant isotope: 14 16 32 16 32 N (99. 63% natural abundance), O (99. 76%), and S (95. 02%), with O, S, and 34 14 S (4. 21%) NMR silent. N has a nuclear moment I = 1 and a sizeable quadrupolar moment that makes the NMR signals usually very broad and dif cult to analyse.


Phosphorus-31 NMR Spectroscopy Related Books

Phosphorus-31 NMR Spectroscopy
Language: en
Pages: 138
Authors: Olaf Kühl
Categories: Science
Type: BOOK - Published: 2008-08-22 - Publisher: Springer Science & Business Media

DOWNLOAD EBOOK

Nuclear Magnetic Resonance is a powerful tool, especially for the identification of 1 13 hitherto unknown organic compounds. H- and C-NMR spectroscopy is known
Phosphorus-31 NMR Spectral Properties in Compound Characterization and Structural Analysis
Language: en
Pages: 480
Authors: Louis D. Quin
Categories: Science
Type: BOOK - Published: 1994-10-27 - Publisher: Wiley-VCH

DOWNLOAD EBOOK

This is a methods-oriented book, which contains enormous amounts of information on 31P NMR, in a concise and well-edited format. It is an invaluable resource fo
Phosphorous-31 NMR
Language: en
Pages: 619
Authors: David G. Gorenstein
Categories: Science
Type: BOOK - Published: 2012-12-02 - Publisher: Academic Press

DOWNLOAD EBOOK

Phosphorous-31 NMR: Principles and Applications focuses on the evolution of phosphorus-31 nuclear magnetic resonance (NMR) as a widely applied spectroscopic pro
Phosphorus-31 NMR Spectroscopy in Stereochemical Analysis
Language: en
Pages: 746
Authors: John G. Verkade
Categories: Science
Type: BOOK - Published: 1987 - Publisher: Wiley-VCH

DOWNLOAD EBOOK

Handbook of Phosphorus-31 Nuclear Magnetic Resonance Data (1990)
Language: en
Pages: 846
Authors: John C. Tebby
Categories: Science
Type: BOOK - Published: 2017-11-22 - Publisher: CRC Press

DOWNLOAD EBOOK

To fully utilize Nuclear Magnetic Resonance (NMR) spectroscopy, a comprehensive and well-organized compilation of NMR data is necessary. While compilations have